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Document Record Detail

Full Document:
RCRA Online Number:12213
Organization of Recipient:EPA
Description: The spot-check program to collect samples to verify delisting petition data is discussed. A recommendation that audit cylinders containing organic compounds be used during all source measurement programs is provided. Problems with spike recovery for metals in Method 3030 - Acid Digestion of Oils, Greases, and Waxes and pH adjustment for the extraction procedure (EP) are outlined. Materials that do not pass through 0.45 um filter are solids and must be extracted. The pH of oil and grease is discussed. It is impossible to determine the pH of non-aqueous materials. Unless specifically stated in the method, results are to be reported “as received,” and a sample is not dried before analysis.
Regulatory Citation(s) : 260.11, 260.22, 261.24 EXIT disclaimer
Statutory Citation(s):NA Read US Code 42, Chapter 82 EXIT disclaimer
Topic(s):Characteristic Wastes; delisting Petitions; Hazardous Waste; Hazardous Waste Recycling; Petitions; Test Methods; Toxicity Characteristic
Approximate Number of Hardcopy Pages:4
EPA Publication Number:NA
RPPC Number (if applicable): 9445.1984(01)
Official OSW Policy:No


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